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Information card for entry 4089283
Preview
| Coordinates | 4089283.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C114 H172 Al2 N4 O3 Si2 |
|---|---|
| Calculated formula | C114 H172 Al2 N4 O3 Si2 |
| Title of publication | Yttrium and Aluminum Alkyl Complexes of a Rigid Bis-Anilido NON-Donor Ligand: Synthesis and Hydroamination Catalysis |
| Authors of publication | Motolko, Kelly S. A.; Emslie, David J. H.; Jenkins, Hilary A. |
| Journal of publication | Organometallics |
| Year of publication | 2017 |
| Journal volume | 36 |
| Journal issue | 8 |
| Pages of publication | 1601 |
| a | 19.33 ± 0.002 Å |
| b | 29.736 ± 0.002 Å |
| c | 20.4953 ± 0.0014 Å |
| α | 90° |
| β | 108.901 ± 0.002° |
| γ | 90° |
| Cell volume | 11145.4 ± 1.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | I 1 2/a 1 |
| Hall space group symbol | -I 2ya |
| Residual factor for all reflections | 0.0842 |
| Residual factor for significantly intense reflections | 0.0522 |
| Weighted residual factors for significantly intense reflections | 0.1249 |
| Weighted residual factors for all reflections included in the refinement | 0.1427 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288470 (current) | 2023-12-21 | Removed the substring '# END of CIF' from the '_shelx_hkl_checksum' data item value in entry 4089283. This modification resulted in a correct checksum value. |
4089283.cif |
| 238087 | 2019-11-24 | cif/ Adding structures of 4089281, 4089282, 4089283 via cif-deposit CGI script. |
4089283.cif |
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Users of the data should acknowledge the original authors of the
structural data.