Crystallography Open Database

Information card for entry 4103257

Preview

Coordinates	4103257.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18.5 H18.5 Ce Cl
Calculated formula	C18.5 H18.5 Ce Cl
Title of publication	Facile Access to Tetravalent Cerium Compounds: One-Electron Oxidation Using Iodine(III) Reagents
Authors of publication	Peter Dröse; Alan R. Crozier; Samira Lashkari; Jochen Gottfriedsen; Steffen Blaurock; Cristian G. Hrib; Cäcilia Maichle-Mössmer; Christoph Schädle; Reiner Anwander; Frank T. Edelmann
Journal of publication	Journal of the American Chemical Society
Year of publication	2010
Journal volume	132
Pages of publication	14046 - 14047
a	8.3124 ± 0.0003 Å
b	14.3667 ± 0.0004 Å
c	13.382 ± 0.0005 Å
α	90°
β	91.514 ± 0.003°
γ	90°
Cell volume	1597.54 ± 0.09 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0327
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0518
Weighted residual factors for all reflections included in the refinement	0.0535
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4103257.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4103257.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4103257.cif
26216	2011-09-19	../uploads/cif-deposit/cod/cif Adding structures of 4103257 via cif-deposit CGI script.	4103257.cif