Crystallography Open Database

Information card for entry 4103827

Preview

Coordinates	4103827.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H42 Ge N2 O2
Calculated formula	C30 H42 Ge N2 O2
Title of publication	A Germanium(II) Hydride as an Effective Reagent for Hydrogermylation Reactions
Authors of publication	Anukul Jana; Debajyoti Ghoshal; Herbert W. Roesky; Ina Objartel; Gerald Schwab; Dietmar Stalke
Journal of publication	Journal of the American Chemical Society
Year of publication	2009
Journal volume	131
Pages of publication	1288 - 1293
a	8.7449 ± 0.0012 Å
b	11.7058 ± 0.0016 Å
c	14.97 ± 0.002 Å
α	98.446 ± 0.002°
β	96.896 ± 0.002°
γ	109.595 ± 0.003°
Cell volume	1404.2 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0354
Residual factor for significantly intense reflections	0.0342
Weighted residual factors for significantly intense reflections	0.087
Weighted residual factors for all reflections included in the refinement	0.0876
Goodness-of-fit parameter for all reflections included in the refinement	1.136
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178784 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/38.	4103827.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4103827.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4103827.cif
28302	2011-10-24	../uploads/cif-deposit/cod/cif Adding structures of 4103827 via cif-deposit CGI script.	4103827.cif