Crystallography Open Database

Information card for entry 4107729

Preview

Coordinates	4107729.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H37 N5 O Sn3
Calculated formula	C29 H37 N5 O Sn3
SMILES	[Sn]12[O]3[Sn]4[N]5([Sn]63[N]2(c2c(N1CC(C)(C)C)cccc2)Cc1[n]6c(ccc1)C5)c1c(N4CC(C)(C)C)cccc1
Title of publication	Trapping of Tin(II) and Lead(II) Homologues of Carbon Monoxide by a Benzannulated Lutidine-Bridged Bisstannylene
Authors of publication	Alexander V. Zabula; Tania Pape; Alexander Hepp; Falko M. Schappacher; Ute Ch. Rodewald; Rainer Pöttgen; F. Ekkehardt Hahn
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	5648 - 5649
a	11.331 ± 0.003 Å
b	17.97 ± 0.004 Å
c	15.809 ± 0.003 Å
α	90°
β	110.63 ± 0.004°
γ	90°
Cell volume	3012.6 ± 1.2 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.079
Weighted residual factors for all reflections included in the refinement	0.0843
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178823 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/77.	4107729.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4107729.cif
55878	2012-05-07	cif/ Adding structures of 4107729 via cif-deposit CGI script.	4107729.cif