Crystallography Open Database

Information card for entry 4109606

Preview

Coordinates	4109606.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C94.5 H93 Cl5 F10 P4 Pt2
Calculated formula	C94.519 H93 Cl5 F10 P4 Pt2
Title of publication	sp Carbon Chains Surrounded by sp3 Carbon Double Helices: Coordination-Driven Self-Assembly of Wirelike Pt(C\τbC)nPt Moieties That Are Spanned by Two P(CH2)mP Linkages
Authors of publication	Jürgen Stahl; Wolfgang Mohr; Laura de Quadras; Thomas B. Peters; James C. Bohling; José Miguel Martín-Alvarez; Gareth R. Owen; Frank Hampel; John A. Gladysz
Journal of publication	Journal of the American Chemical Society
Year of publication	2007
Journal volume	129
Pages of publication	8282 - 8295
a	10.9876 ± 0.0001 Å
b	17.2761 ± 0.0002 Å
c	24.8047 ± 0.0002 Å
α	77.828 ± 0.0006°
β	79.3644 ± 0.0006°
γ	87.8733 ± 0.0005°
Cell volume	4523.57 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0482
Residual factor for significantly intense reflections	0.0396
Weighted residual factors for significantly intense reflections	0.104
Weighted residual factors for all reflections included in the refinement	0.1117
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4109606.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4109606.cif
58383	2012-05-28	cif/ Adding structures of 4109606 via cif-deposit CGI script.	4109606.cif