Crystallography Open Database

Information card for entry 4110496

Preview

Coordinates	4110496.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H55 N Si5
Calculated formula	C27 H55 N Si5
Title of publication	Synthesis, Structure, and Bonding of Stable Dialkylsilaketenimines
Authors of publication	Takashi Abe; Takeaki Iwamoto; Chizuko Kabuto; Mitsuo Kira
Journal of publication	Journal of the American Chemical Society
Year of publication	2006
Journal volume	128
Pages of publication	4228 - 4229
a	11.2882 ± 0.0007 Å
b	13.2925 ± 0.0007 Å
c	22.3203 ± 0.0015 Å
α	90 ± 0.001°
β	98.459 ± 0.001°
γ	90 ± 0.001°
Cell volume	3312.7 ± 0.3 Å³
Cell temperature	200.15 K
Ambient diffraction temperature	200.15 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.06
Residual factor for significantly intense reflections	0.0572
Weighted residual factors for significantly intense reflections	0.1372
Weighted residual factors for all reflections included in the refinement	0.1383
Goodness-of-fit parameter for all reflections included in the refinement	1.31
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178875 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/04.	4110496.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4110496.cif
59295	2012-06-05	cif/ Adding structures of 4110496 via cif-deposit CGI script.	4110496.cif