Crystallography Open Database

Information card for entry 4112151

Preview

Coordinates	4112151.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	compound 2
Formula	C30 H49 Ag B11 P
Calculated formula	C30 H49 Ag B11 P
Title of publication	Silver-Phosphine Complexes of the Highly Methylated Carborane Monoanion [closo-1-H-CB11Me11]-
Authors of publication	Adam J. Clarke; Michael J. Ingleson; Gabriele Kociok-Köhn; Mary F. Mahon; Nathan J. Patmore; Jonathan P. Rourke; Giuseppe D. Ruggiero; Andrew S. Weller
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	1503 - 1517
a	9.184 ± 0.0001 Å
b	13.617 ± 0.0002 Å
c	15.152 ± 0.0003 Å
α	111.637 ± 0.001°
β	95.005 ± 0.001°
γ	100.336 ± 0.001°
Cell volume	1708.23 ± 0.05 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0627
Residual factor for significantly intense reflections	0.0378
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.1043
Goodness-of-fit parameter for all reflections included in the refinement	1.017
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178892 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/21.	4112151.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4112151.cif
64516	2012-08-19	cif/ Adding structures of 4112151 via cif-deposit CGI script.	4112151.cif