Crystallography Open Database

Information card for entry 4113527

Preview

Coordinates	4113527.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H43 Dy I3 N13
Calculated formula	C26 H46 Dy I3 N13
Title of publication	A Novel Bis(imino)amine Ligand as a Result of Acetonitrile Coupling with the Diiodides of Dy(II) and Tm(II)
Authors of publication	Mikhail N. Bochkarev; Georgii V. Khoroshenkov; Herbert Schumann; Sebastian Dechert
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	2894 - 2895
a	20.3218 ± 0.0003 Å
b	13.8313 ± 0.0001 Å
c	15.4992 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	4356.47 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0594
Residual factor for significantly intense reflections	0.0419
Weighted residual factors for significantly intense reflections	0.0916
Weighted residual factors for all reflections included in the refinement	0.0995
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178906 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/35.	4113527.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4113527.cif
66783	2012-09-13	cif/ Adding structures of 4113527 via cif-deposit CGI script.	4113527.cif