Crystallography Open Database

Information card for entry 4114186

Preview

Coordinates	4114186.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Dipp*SnCl]~2~
Formula	C60 H74 Cl2 Sn2
Calculated formula	C60 H74 Cl2 Sn2
Title of publication	Germanium and Tin Analogues of Alkynes and Their Reduction Products
Authors of publication	Lihung Pu; Andrew D. Phillips; Anne F. Richards; Matthias Stender; Richard S. Simons; Marilyn M. Olmstead; Philip P. Power
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	11626 - 11636
a	13.3297 ± 0.0007 Å
b	14.1189 ± 0.0009 Å
c	14.4249 ± 0.001 Å
α	90°
β	97.247 ± 0.003°
γ	90°
Cell volume	2693.1 ± 0.3 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0771
Residual factor for significantly intense reflections	0.0697
Weighted residual factors for significantly intense reflections	0.192
Weighted residual factors for all reflections included in the refinement	0.1997
Goodness-of-fit parameter for all reflections included in the refinement	1.076
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178912 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/41.	4114186.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4114186.cif
67469	2012-09-26	cif/ Adding structures of 4114186 via cif-deposit CGI script.	4114186.cif