Crystallography Open Database

Information card for entry 4115942

Preview

Coordinates	4115942.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H29 N Si Sn
Calculated formula	C27 N Si Sn
Title of publication	Structures of [(Amino)phenylsilyl]lithiums and Related Compounds in Solution and in the Solid State
Authors of publication	Atsushi Kawachi; Kohei Tamao
Journal of publication	Journal of the American Chemical Society
Year of publication	2000
Journal volume	122
Pages of publication	1919 - 1926
a	10.413 ± 0.002 Å
b	12.8154 ± 0.0007 Å
c	9.74 ± 0.002 Å
α	97.081 ± 0.01°
β	92.01 ± 0.02°
γ	86.315 ± 0.008°
Cell volume	1286.7 ± 0.4 Å³
Cell temperature	293.2 K
Ambient diffraction temperature	293.2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0421
Weighted residual factors for significantly intense reflections	0.0697
Weighted residual factors for all reflections included in the refinement	0.0697
Goodness-of-fit parameter for all reflections included in the refinement	1.547
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4115942.cif
120077	2014-07-12	Adding DOIs to range 4/11 structures.	4115942.cif
70506	2012-12-26	cif/ Adding structures of 4115942 via cif-deposit CGI script.	4115942.cif