Crystallography Open Database

Information card for entry 4116357

Preview

Coordinates	4116357.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C4 H12 O2 Sn
Calculated formula	C8 H24 O4 Sn2
Title of publication	Reaction of Dialkyltin Methoxide with Carbon Dioxide Relevant to the Mechanism of Catalytic Carbonate Synthesis
Authors of publication	Jun-Chul Choi; Toshiyasu Sakakura; Takeshi Sako
Journal of publication	Journal of the American Chemical Society
Year of publication	1999
Journal volume	121
Pages of publication	3793 - 3794
a	8.03 ± 0.01 Å
b	8.162 ± 0.006 Å
c	11.375 ± 0.008 Å
α	90.02 ± 0.07°
β	91.78 ± 0.08°
γ	89.98 ± 0.1°
Cell volume	745.2 ± 1.2 Å³
Cell temperature	243.2 K
Ambient diffraction temperature	243.2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0512
Residual factor for significantly intense reflections	0.0512
Weighted residual factors for significantly intense reflections	0.079
Weighted residual factors for all reflections included in the refinement	0.079
Goodness-of-fit parameter for all reflections included in the refinement	1.86
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178934 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/63.	4116357.cif
70970	2013-01-13	cif/ Adding structures of 4116357 via cif-deposit CGI script.	4116357.cif