Crystallography Open Database

Information card for entry 4116564

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Coordinates	4116564.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H40 Cl2 Ga2 N4
Calculated formula	C20 H40 Cl2 Ga2 N4
Title of publication	A Carbene Analogue with Low-Valent Gallium as a Heteroatom in a quasi-Aromatic Imidazolate Anion
Authors of publication	Eva S. Schmidt; Alexander Jockisch; Hubert Schmidbaur
Journal of publication	Journal of the American Chemical Society
Year of publication	1999
Journal volume	121
Pages of publication	9758 - 9759
a	61.445 ± 0.013 Å
b	10.441 ± 0.001 Å
c	29.371 ± 0.01 Å
α	90°
β	101.45 ± 0.01°
γ	90°
Cell volume	18468 ± 8 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1172
Residual factor for significantly intense reflections	0.0615
Weighted residual factors for significantly intense reflections	0.1286
Weighted residual factors for all reflections included in the refinement	0.1436
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178936 (current)	2016-03-22	cif/4/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/11/65.	4116564.cif
72690	2013-01-26	cif/ Adding structures of 4116564 via cif-deposit CGI script.	4116564.cif