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Information card for entry 4129954
Preview
| Coordinates | 4129954.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H30 F6 N3 O3 Rh Sb |
|---|---|
| Calculated formula | C24 H30 F6 N3 O3 Rh Sb |
| Title of publication | A Stable Coordination Complex of Rh(IV) in an N,O-Donor Environment. |
| Authors of publication | Sinha, Shashi B.; Shopov, Dimitar Y.; Sharninghausen, Liam S.; Vinyard, David J.; Mercado, Brandon Q.; Brudvig, Gary W.; Crabtree, Robert H. |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 2015 |
| Journal volume | 137 |
| Journal issue | 50 |
| Pages of publication | 15692 - 15695 |
| a | 14.7512 ± 0.001 Å |
| b | 33.1199 ± 0.0006 Å |
| c | 12.0932 ± 0.0002 Å |
| α | 90° |
| β | 103.836 ± 0.007° |
| γ | 90° |
| Cell volume | 5736.8 ± 0.4 Å3 |
| Cell temperature | 93 ± 2 K |
| Ambient diffraction temperature | 93 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.064 |
| Residual factor for significantly intense reflections | 0.0555 |
| Weighted residual factors for significantly intense reflections | 0.125 |
| Weighted residual factors for all reflections included in the refinement | 0.1298 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.128 |
| Diffraction radiation wavelength | 1.54187 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 240571 (current) | 2019-11-25 | cif/ Adding structures of 4129954 via cif-deposit CGI script. |
4129954.cif |
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