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Information card for entry 4301573
Preview
Coordinates | 4301573.cif |
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Original paper (by DOI) | HTML |
Formula | C57 H58 Mo N2 P4 |
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Calculated formula | C57 H58 Mo N2 P4 |
Title of publication | Structural, Spectroscopic, and Kinetic Investigation of the Molybdenum Dialkylhydrazido Complexes [MoBr(NNC5H10)(dppe)2]Br and [Mo(NNC5H10)(dppe)2]: Activation Parameters and Revised Mechanism for N-N Cleavage |
Authors of publication | Ameli Dreher; Klaus Mersmann; Christian Näther; Ivana Ivanovic-Burmazovic; Rudi van Eldik; Felix Tuczek |
Journal of publication | Inorganic Chemistry |
Year of publication | 2009 |
Journal volume | 48 |
Pages of publication | 2078 - 2093 |
a | 16.3478 ± 0.0013 Å |
b | 19.9745 ± 0.0016 Å |
c | 16.6728 ± 0.0013 Å |
α | 90° |
β | 108.954 ± 0.009° |
γ | 90° |
Cell volume | 5149.1 ± 0.8 Å3 |
Cell temperature | 220 ± 2 K |
Ambient diffraction temperature | 220 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0395 |
Residual factor for significantly intense reflections | 0.0327 |
Weighted residual factors for significantly intense reflections | 0.0836 |
Weighted residual factors for all reflections included in the refinement | 0.0863 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
179053 (current) | 2016-03-22 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/15. |
4301573.cif |
120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4301573.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4301573.cif |
31985 | 2012-01-04 | cif/ Canging data item '_diffrn_standards_decay_% none' to '_diffrn_standards_decay_% 0'. |
4301573.cif |
1054 | 2010-03-28 | cif/4/ Adding data extracted in Inorg-Chem-2009_01-10/ processing. |
4301573.cif |
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Users of the data should acknowledge the original authors of the
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