Crystallography Open Database

Information card for entry 4302265

Preview

Coordinates	4302265.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 Al N P2
Calculated formula	C32 H38 Al N P2
SMILES	C(C)(C)[P]1(C(C)C)c2ccccc2N2c3ccccc3[P](c3ccccc3)(c3ccccc3)[Al]12(C)C
Title of publication	Synthesis and Structural Characterization of Five-Coordinate Aluminum Complexes Containing Diarylamido Diphosphine Ligands
Authors of publication	Lee, Pei-Ying; Liang, Lan-Chang
Journal of publication	Inorganic chemistry
Year of publication	2009
Journal volume	48
Journal issue	12
Pages of publication	5480 - 5487
a	9.4805 ± 0.0003 Å
b	11.5257 ± 0.0003 Å
c	16.65 ± 0.0006 Å
α	108.584 ± 0.002°
β	96.379 ± 0.002°
γ	107.357 ± 0.002°
Cell volume	1602.63 ± 0.09 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1316
Residual factor for significantly intense reflections	0.0767
Weighted residual factors for significantly intense reflections	0.2232
Weighted residual factors for all reflections included in the refinement	0.2612
Goodness-of-fit parameter for all reflections included in the refinement	0.847
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	4338631
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
210021 (current)	2018-08-21	cif/4/ Updating bibliography in entries 4302263-4302269, 4338629-4338635. Marking entries 4302263-4302269 as duplicates of entries 4338629-4338635.	4302265.cif
179060	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/22.	4302265.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4302265.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4302265.cif