Crystallography Open Database

Information card for entry 4303628

Preview

Coordinates	4303628.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tetrabuthylammonium-pentachloridoindazoleosmate(IV)
Formula	C23 H42 Cl5 N3 Os
Calculated formula	C23 H42 Cl5 N3 Os
Title of publication	[OsIVCl5(Hazole)]- Complexes: Synthesis, Structure, Spectroscopic Properties, and Antiproliferative Activity
Authors of publication	Gabriel E. Büchel; Iryna N. Stepanenko; Michaela Hejl; Michael A. Jakupec; Vladimir B. Arion; Bernhard K. Keppler
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	10737 - 10747
a	9.8278 ± 0.0008 Å
b	10.9541 ± 0.0008 Å
c	14.7537 ± 0.0012 Å
α	109.992 ± 0.005°
β	96.282 ± 0.006°
γ	91.468 ± 0.005°
Cell volume	1480.3 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0427
Residual factor for significantly intense reflections	0.0282
Weighted residual factors for significantly intense reflections	0.0558
Weighted residual factors for all reflections included in the refinement	0.06
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179074 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/36.	4303628.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4303628.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4303628.cif
1125	2010-04-25	cif/4/ Adding CIFs for the Inorg-Chem-2009_11-24 deposition.	4303628.cif