Crystallography Open Database

Information card for entry 4304205

Preview

Coordinates	4304205.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H51 Br N2 Ni P2 Si
Calculated formula	C22 H47 Br N2 Ni P2 Si
Title of publication	First-Row Transition Metal-Halide Complexes Supported by a Monoanionic [N2P2] Ligand
Authors of publication	Wayne A. Chomitz; Seth F. Mickenberg; John Arnold
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	373 - 380
a	16.555 ± 0.003 Å
b	11.593 ± 0.002 Å
c	14.908 ± 0.003 Å
α	90°
β	92.564 ± 0.003°
γ	90°
Cell volume	2858.3 ± 0.9 Å³
Cell temperature	156 ± 2 K
Ambient diffraction temperature	156 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0815
Residual factor for significantly intense reflections	0.0467
Weighted residual factors for significantly intense reflections	0.1001
Weighted residual factors for all reflections included in the refinement	0.1076
Goodness-of-fit parameter for all reflections included in the refinement	1.175
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179080 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/42.	4304205.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304205.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304205.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304205.cif