Crystallography Open Database

Information card for entry 4304357

Preview

Coordinates	4304357.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H29 N2 Ni P
Calculated formula	C32 H29 N2 Ni P
SMILES	[Ni]1([P](c2ccccc2)(c2ccccc2)C=C(N1c1ccccc1)C)([n]1ccccc1)c1ccccc1
Title of publication	Nickel(II) Complexes Containing Bidentate Amido Phosphine Ligands Derived from α-Iminophosphorus Ylides: Synthesis and Structural Characterization
Authors of publication	Pei-Ying Lee; Lan-Chang Liang
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	749 - 758
a	10.238 ± 0.0004 Å
b	9.748 ± 0.0005 Å
c	26.779 ± 0.0014 Å
α	90°
β	91.737 ± 0.002°
γ	90°
Cell volume	2671.3 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1099
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.1372
Weighted residual factors for all reflections included in the refinement	0.1619
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179081 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/43.	4304357.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4304357.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4304357.cif
1163	2010-05-11	cif/4/: committing data from the Inorg-Chem-2008_01-12/ deposition.	4304357.cif