Crystallography Open Database

Information card for entry 4305800

Preview

Coordinates	4305800.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H38 F6 N6 O P Ru
Calculated formula	C18 H36 F6 N6 O P Ru
Title of publication	Spectroscopic Studies and Structures of trans-Ruthenium(II) and Ruthenium(III) Bis(cyanide) Complexes Supported by a Tetradentate Macrocyclic Tertiary Amine Ligand
Authors of publication	Chun-Yuen Wong; Fu-Wa Lee; Chi-Ming Che; Yung Fong Cheng; David Lee Phillips; Nianyong Zhu
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	10308 - 10316
a	22.722 ± 0.004 Å
b	12.625 ± 0.002 Å
c	10.199 ± 0.002 Å
α	90°
β	116.25 ± 0.02°
γ	90°
Cell volume	2624 ± 0.9 Å³
Cell temperature	301 ± 2 K
Ambient diffraction temperature	301 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0538
Residual factor for significantly intense reflections	0.044
Weighted residual factors for significantly intense reflections	0.1315
Weighted residual factors for all reflections included in the refinement	0.1389
Goodness-of-fit parameter for all reflections included in the refinement	1.182
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179096 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/58.	4305800.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4305800.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4305800.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4305800.cif