Crystallography Open Database

Information card for entry 4306197

Preview

Coordinates	4306197.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H28 Cu F7 N5 O2 V2
Calculated formula	C22 H28 Cu F7 N5 O2 V2
Title of publication	Hydrothermal Synthesis of Vanadium Oxyfluoride Chains Incorporating Covalently Bound Copper Coordination Complexes
Authors of publication	Thushitha Mahenthirarajah; Yang Li; Philip Lightfoot
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	9097 - 9102
a	8.981 ± 0.003 Å
b	13.533 ± 0.006 Å
c	13.545 ± 0.006 Å
α	89.15 ± 0.03°
β	70.64 ± 0.02°
γ	74.19 ± 0.03°
Cell volume	1489.2 ± 1.1 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.14
Residual factor for significantly intense reflections	0.1236
Weighted residual factors for significantly intense reflections	0.3216
Weighted residual factors for all reflections included in the refinement	0.3388
Goodness-of-fit parameter for all reflections included in the refinement	1.083
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4306197.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306197.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306197.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306197.cif