Crystallography Open Database

Information card for entry 4307177

Preview

Coordinates	4307177.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	catena-bis[(2,2'bipyridine)-copper(II)]-(aquo)-(perchlorate) -(mu4-adipato,O,O',O'',O''') perchlorate hydrated
Formula	C26 H28 Cl2 Cu2 N4 O14
Calculated formula	C26 H28 Cl2 Cu2 N4 O14
Title of publication	Syntheses, Crystal Structures, and Magnetic Properties of Metal-Organic Hybrid Materials of Cu(II): Effect of a Long Chain Dicarboxylate Backbone, and Counteranion in Their Structural Diversity
Authors of publication	A. K. Ghosh; D. Ghoshal; E. Zangrando; J. Ribas; N. Ray Chaudhuri
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	3057 - 3071
a	15.01 ± 0.003 Å
b	11.733 ± 0.001 Å
c	18.454 ± 0.003 Å
α	90°
β	95.374 ± 0.002°
γ	90°
Cell volume	3235.7 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.2487
Residual factor for significantly intense reflections	0.0538
Weighted residual factors for significantly intense reflections	0.0986
Weighted residual factors for all reflections included in the refinement	0.1266
Goodness-of-fit parameter for all reflections included in the refinement	0.906
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Mokα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179109 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/71.	4307177.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307177.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307177.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307177.cif