Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4309334
Preview
| Coordinates | 4309334.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | Co5 H12 Na10 O6 S20 Sn5 |
|---|---|
| Calculated formula | Co4.98 Na10 O6 S20 Sn5.02 |
| Title of publication | Unusual Syntheses, Structures, and Electronic Properties of Compounds Containing Ternary, T3-Type Supertetrahedral M/Sn/S Anions [M5Sn(μ3-S)4(SnS4)4]10- (M = Zn, Co) |
| Authors of publication | Christian Zimmermann; Christopher E. Anson; Florian Weigend; Rodolphe Clérac; Stefanie Dehnen |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 5686 - 5695 |
| a | 13.436 ± 0.002 Å |
| b | 13.57 ± 0.002 Å |
| c | 14.105 ± 0.002 Å |
| α | 95.77 ± 0.003° |
| β | 117.889 ± 0.003° |
| γ | 98.364 ± 0.003° |
| Cell volume | 2206.7 ± 0.6 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1179 |
| Residual factor for significantly intense reflections | 0.0676 |
| Weighted residual factors for significantly intense reflections | 0.1523 |
| Weighted residual factors for all reflections included in the refinement | 0.1822 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 194044 (current) | 2017-03-07 | cif/4/30/93/ (antanas@echidna.ibt.lt) Removing the '_pupl_author_name' data item from entries 4309332, 4309333, 4309334 since it was not found in the core CIF dictionary and the same information was already provided in the official bibliography data items. No information was lost by removing this data item. Changing data name '_publ_author_adress' to '_publ_author_address' and moving the data item to the '_publ_author' loop. |
4309334.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4309334.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4309334.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4309334.cif |
| 1526 | 2010-09-26 | cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming). |
4309334.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.