Crystallography Open Database

Information card for entry 4310102

Preview

Coordinates	4310102.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H96 K3.5 N0.5 O63.5 Si V2 W10
Calculated formula	C46 K3.5 N0.5 O63.5 Si V2 W10
Title of publication	Reactivity of Bis(μ-hydroxo) Divanadium Site in γ-H2SiV2W10O404- with Hydroxo Compounds
Authors of publication	Yoshinao Nakagawa; Kazuhiro Uehara; Noritaka Mizuno
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	9068 - 9075
a	15.107 ± 0.007 Å
b	17.44 ± 0.008 Å
c	21.742 ± 0.012 Å
α	81.44 ± 0.02°
β	84.21 ± 0.02°
γ	67.64 ± 0.02°
Cell volume	5232 ± 5 Å³
Cell temperature	183.1 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.064
Weighted residual factors for all reflections included in the refinement	0.073
Goodness-of-fit parameter for all reflections included in the refinement	4.079
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4310102.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310102.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310102.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4310102.cif