Crystallography Open Database

Information card for entry 4310484

Preview

Coordinates	4310484.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35.5 H39.25 Ag2 F12 N14.25 O2.25 Sb2
Calculated formula	C35.5 H39.25 Ag2 F12 N14.25 O2.25 Sb2
Title of publication	Supramolecular Structural Variations with Changes in Anion and Solvent in Silver(I) Complexes of a Semirigid, Bitopic Tris(pyrazolyl)methane Ligand
Authors of publication	Daniel L. Reger; Radu F. Semeniuc; Vitaly Rassolov; Mark D. Smith
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	537 - 554
a	10.4341 ± 0.0006 Å
b	15.4008 ± 0.0009 Å
c	15.8447 ± 0.0009 Å
α	77.724 ± 0.001°
β	77.412 ± 0.001°
γ	78.326 ± 0.001°
Cell volume	2395.4 ± 0.2 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.042
Residual factor for significantly intense reflections	0.0339
Weighted residual factors for significantly intense reflections	0.0771
Weighted residual factors for all reflections included in the refinement	0.0791
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4310484.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4310484.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4310484.cif
1972	2010-11-07	../uploads/cif-deposit/cod/cif Adding structures of 4310484 via cif-deposit CGI script.	4310484.cif