Crystallography Open Database

Information card for entry 4311414

Preview

Coordinates	4311414.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25.33 H29.5 I3 La N11.17
Calculated formula	C25.3333 H29.5 I3 La N11.1667
Title of publication	Comparative Structural Studies of Iodide Complexes of Uranium(III) and Lanthanide(III) with Hexadentate Tetrapodal Neutral N-Donor Ligands
Authors of publication	Lydia Karmazin; Marinella Mazzanti; Jean-Philippe Bezombes; Christelle Gateau; Jacques Pécaut
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	5147 - 5158
a	33.6224 ± 0.0011 Å
b	33.6224 ± 0.0011 Å
c	15.2549 ± 0.0007 Å
α	90°
β	90°
γ	120°
Cell volume	14934.7 ± 1 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	161
Hermann-Mauguin space group symbol	R 3 c :H
Hall space group symbol	R 3 -2"c
Residual factor for all reflections	0.0267
Residual factor for significantly intense reflections	0.0216
Weighted residual factors for significantly intense reflections	0.0476
Weighted residual factors for all reflections included in the refinement	0.0486
Goodness-of-fit parameter for all reflections included in the refinement	0.999
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4311414.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4311414.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4311414.cif
2913	2010-11-13	../uploads/cif-deposit/cod/cif Adding structures of 4311414 via cif-deposit CGI script.	4311414.cif