Crystallography Open Database

Information card for entry 4312549

Preview

Coordinates	4312549.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49 H34 B2 Cl2 F8 O8 P4 Pd
Calculated formula	C49 H34 B2 Cl2 F8 O8 P4 Pd
Title of publication	Enolphosphato-Phosphines: A New Class of P,O Ligands
Authors of publication	Xavier Morise; Pierre Braunstein; Richard Welter
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	7752 - 7765
a	17.133 Å
b	22.051 Å
c	14.681 Å
α	90°
β	90°
γ	90°
Cell volume	5546.48 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	52
Hermann-Mauguin space group symbol	P n n a
Hall space group symbol	-P 2a 2bc
Residual factor for all reflections	0.0764
Residual factor for significantly intense reflections	0.0582
Weighted residual factors for significantly intense reflections	0.1615
Weighted residual factors for all reflections included in the refinement	0.1845
Goodness-of-fit parameter for all reflections included in the refinement	0.921
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179164 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/25.	4312549.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4312549.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4312549.cif
5562	2011-01-05	../uploads/cif-deposit/cod/cif Adding structures of 4312549 via cif-deposit CGI script.	4312549.cif