Crystallography Open Database

Information card for entry 4313037

Preview

Coordinates	4313037.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H40 N4 O Rh2 S4
Calculated formula	C46 H36 N4 O2 Rh2 S4
Title of publication	Isolation of the Novel Dirhodium(II/II) Thiolate Compound Rh2(η1-C6H5S)2(μ-C6H5S)2(bpy)2
Authors of publication	Karn Sorasaenee; José Ramón Galán-Mascarós; Kim R. Dunbar
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	661 - 663
a	20.398 ± 0.004 Å
b	11.861 ± 0.002 Å
c	17.417 ± 0.004 Å
α	90°
β	108.98 ± 0.03°
γ	90°
Cell volume	3984.8 ± 1.6 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1796
Residual factor for significantly intense reflections	0.0756
Weighted residual factors for significantly intense reflections	0.1424
Weighted residual factors for all reflections included in the refinement	0.2928
Goodness-of-fit parameter for all reflections included in the refinement	0.98
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179183 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/30.	4313037.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313037.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313037.cif
6106	2011-01-10	../uploads/cif-deposit/cod/cif Adding structures of 4313037 via cif-deposit CGI script.	4313037.cif