Crystallography Open Database

Information card for entry 4313343

Preview

Coordinates	4313343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Cs5 Eu O50 Si W11
Calculated formula	Cs4.99 Eu O50 Si W11
Title of publication	Solid-State and Solution Studies of {Lnn(SiW11O39)} Polyoxoanions: An Example of Building Block Condensation Dependent on the Nature of the Rare Earth
Authors of publication	Pierre Mialane; Laurent Lisnard; Alain Mallard; Jérôme Marrot; Elisabeth Antic-Fidancev; Patrick Aschehoug; Daniel Vivien; Francis Sécheresse
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	2102 - 2108
a	11.5262 ± 0.0004 Å
b	22.3425 ± 0.0007 Å
c	18.9907 ± 0.0006 Å
α	90°
β	100.347 ± 0.001°
γ	90°
Cell volume	4811 ± 0.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0634
Residual factor for significantly intense reflections	0.0387
Weighted residual factors for significantly intense reflections	0.0726
Weighted residual factors for all reflections included in the refinement	0.0807
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179191 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/33.	4313343.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313343.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313343.cif
17004	2011-03-31	cif/ Commiting CIFs, that were updated with the 'cif_fix_values' script, using options '--fix-misspelled replacement_values.lst', '--fix-temperature' and '--fix-enums' with built-in table of enum values. The following cmd was used: > (set -x; find ? -name \*.cif \| sort \| xargs -i sh -c 'if !( > cif_fix_values --fix-misspelled ~/../inputs/replacament_values.lst {} \| > cif_filter --add-cif-header {} \| > sponge {} ) 2>&1 \| grep NOTE; then svn revert {}; > fi' ) &	4313343.cif
6412	2011-01-11	../uploads/cif-deposit/cod/cif Adding structures of 4313343 via cif-deposit CGI script.	4313343.cif