Crystallography Open Database

Information card for entry 4313359

Preview

Coordinates	4313359.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H55 B Cl5 Ga2 Li N2 O4
Calculated formula	C30 H55 B Cl5 Ga2 Li N2 O4
Title of publication	Syntheses and X-ray Structures of Monocyclic, Bicyclic, and Spirocyclic Gallium and Indium Boraamidinates
Authors of publication	Tristram Chivers; Chantall Fedorchuk; Gabriele Schatte; Masood Parvez
Journal of publication	Inorganic Chemistry
Year of publication	2003
Journal volume	42
Pages of publication	2084 - 2093
a	13.9213 ± 0.0013 Å
b	11.6036 ± 0.0011 Å
c	25.361 ± 0.002 Å
α	90°
β	99.0474 ± 0.0019°
γ	90°
Cell volume	4045.8 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0665
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.1005
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179191 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/33.	4313359.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4313359.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4313359.cif
6428	2011-01-11	../uploads/cif-deposit/cod/cif Adding structures of 4313359 via cif-deposit CGI script.	4313359.cif