Crystallography Open Database

Information card for entry 4317980

Preview

Coordinates	4317980.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	[Co(pmp)2]ClO4
Formula	C24 H20 Cl Co N6 O6
Calculated formula	C24 H20 Cl Co N6 O6
Title of publication	Unusual Reactivity of Methylene Group Adjacent to Pyridine-2-Carboxamido Moiety in Iron(III) and Cobalt(III) Complexes
Authors of publication	John M. Rowland; Marilyn M. Olmstead; Pradip K. Mascharak
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	2754 - 2760
a	8.5758 ± 0.0011 Å
b	8.906 ± 0.0012 Å
c	15.49 ± 0.003 Å
α	90°
β	99.77 ± 0.005°
γ	90°
Cell volume	1165.9 ± 0.3 Å³
Cell temperature	91 ± 2 K
Ambient diffraction temperature	91 ± 2 K
Number of distinct elements	6
Space group number	7
Hermann-Mauguin space group symbol	P 1 n 1
Hall space group symbol	P -2yac
Residual factor for all reflections	0.0578
Residual factor for significantly intense reflections	0.0462
Weighted residual factors for significantly intense reflections	0.1092
Weighted residual factors for all reflections included in the refinement	0.1154
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179259 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/79.	4317980.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4317980.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4317980.cif
14266	2011-03-09	../uploads/cif-deposit/cod/cif Adding structures of 4317980 via cif-deposit CGI script.	4317980.cif