Crystallography Open Database

Information card for entry 4318481

Preview

Coordinates	4318481.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H31 Mo12 O66 V7
Calculated formula	Mo12 O66 V7
Title of publication	Hydrothermal Synthesis of the First Vanadomolybdenum Polyoxocation with a "Metal-Bonded" Spherical Framework
Authors of publication	Wenbin Yang; Canzhong Lu; Xiaoping Zhan; Honghui Zhuang
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	4621 - 4623
a	12.7305 ± 0.0018 Å
b	12.7305 ± 0.0018 Å
c	17.788 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	2882.8 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	128
Hermann-Mauguin space group symbol	P 4/m n c
Hall space group symbol	-P 4 2n
Residual factor for all reflections	0.082
Residual factor for significantly intense reflections	0.0686
Weighted residual factors for significantly intense reflections	0.2182
Weighted residual factors for all reflections included in the refinement	0.2265
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179264 (current)	2016-03-23	cif/4/31/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/31/84.	4318481.cif
120093	2014-07-12	Adding DOIs to range 4/31 structures.	4318481.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4318481.cif
15195	2011-03-14	../uploads/cif-deposit/cod/cif Adding structures of 4318481 via cif-deposit CGI script.	4318481.cif