Crystallography Open Database

Information card for entry 4320524

4320523 << 4320524 >> 4320525

Preview

Coordinates	4320524.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C100.8 H77.6 Cl13.6 F16 N12 O16 Rh4
Calculated formula	C100.8 H64 Cl13.6 F16 N12 O16 Rh4
Title of publication	Controlling the Dimensionality of Metal-Metal Bonded Rh24+ Polymers by the Length of the Linker. A Disciplined Example of Crystal Engineering
Authors of publication	F. Albert Cotton; Chun Lin; Carlos A. Murillo
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5886 - 5889
a	11.802 ± 0.001 Å
b	28.303 ± 0.002 Å
c	18.82 ± 0.002 Å
α	90°
β	95.673 ± 0.002°
γ	90°
Cell volume	6255.7 ± 1 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	7
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.1807
Residual factor for significantly intense reflections	0.0948
Weighted residual factors for significantly intense reflections	0.2168
Weighted residual factors for all reflections included in the refinement	0.2571
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4320524.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320524.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320524.cif
17720	2011-04-09	../uploads/cif-deposit/cod/cif Adding structures of 4320524 via cif-deposit CGI script.	4320524.cif