Crystallography Open Database

Information card for entry 4321279

Preview

Coordinates	4321279.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H46 N4 O20 Ru2 S2
Calculated formula	C32 H44 N4 O19 Ru2 S2
Title of publication	Synthesis of Bis-Thiolato-Bridged Ru(III) Dimers. The Crystal Structure of [Ru(H2edta)(μ-SC6H5)]2
Authors of publication	Beth R. Cameron; Gary J. Bridger; Kevin P. Maresca; Jon Zubieta
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	3928 - 3930
a	10.4396 ± 0.0001 Å
b	10.4396 ± 0.0001 Å
c	36.2157 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	3946.98 ± 0.09 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	92
Hermann-Mauguin space group symbol	P 41 21 2
Hall space group symbol	P 4abw 2nw
Residual factor for all reflections	0.0714
Residual factor for significantly intense reflections	0.0635
Weighted residual factors for significantly intense reflections	0.0976
Weighted residual factors for all reflections included in the refinement	0.0998
Goodness-of-fit parameter for all reflections included in the refinement	1.395
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179315 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/12.	4321279.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321279.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321279.cif
18630	2011-05-03	../uploads/cif-deposit/cod/cif Adding structures of 4321279 via cif-deposit CGI script.	4321279.cif