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Information card for entry 4322006
Preview
| Coordinates | 4322006.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H33 Cl2 F3 N2 O4 P2 S W |
|---|---|
| Calculated formula | C104 H132 Cl8 F12 N8 O16 P8 S4 W4 |
| Title of publication | Synthesis and Structures of Tungsten (1-Pyridinio)imido Complexes and Their Facile N-N Bond Cleavage1 |
| Authors of publication | Hiroshige Ishino; Shin'ichi Tokunaga; Hidetake Seino; Youichi Ishii; Masanobu Hidai |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 1999 |
| Journal volume | 38 |
| Pages of publication | 2489 - 2496 |
| a | 8.823 ± 0.004 Å |
| b | 34.939 ± 0.005 Å |
| c | 10.729 ± 0.003 Å |
| α | 90° |
| β | 93.58 ± 0.03° |
| γ | 90° |
| Cell volume | 3300.9 ± 1.8 Å3 |
| Cell temperature | 20 K |
| Ambient diffraction temperature | 20 K |
| Number of distinct elements | 9 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for significantly intense reflections | 0.041 |
| Weighted residual factors for significantly intense reflections | 0.027 |
| Goodness-of-fit parameter for significantly intense reflections | 1.33 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKalpha |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 191073 (current) | 2017-01-29 | cif/4/32/20/ (antanas@kurmis) Changing the values of the _geom_angle_atom_site_label_1, _geom_angle_atom_site_label_2, _geom_angle_atom_site_label_3, _geom_bond_atom_site_label_1 and _geom_bond_atom_site_label_2 data items to match the _atom_site_label data item values in entries 4322005, 4322006, 4322007. |
4322006.cif |
| 179323 | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/20. |
4322006.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4322006.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4322006.cif |
| 19895 | 2011-05-30 | ../uploads/cif-deposit/cod/cif Adding structures of 4322006 via cif-deposit CGI script. |
4322006.cif |
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Users of the data should acknowledge the original authors of the
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