Crystallography Open Database

Information card for entry 4324247

Preview

Coordinates	4324247.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H30 In N6 Ni S7 Sb3
Calculated formula	C9 H30 In N6 Ni S7 Sb3
Title of publication	[M(dap)3]InSb3S7 (M = Co, Ni): Two Novel Open-Framework Thioindate-Thioantimonates with 8-, 12-, and 16-Ring Intersecting Channels
Authors of publication	Jian Zhou; Litao An; Feng Zhang
Journal of publication	Inorganic Chemistry
Year of publication	2011
Journal volume	50
Pages of publication	415 - 417
a	10.668 ± 0.002 Å
b	16.207 ± 0.003 Å
c	18.247 ± 0.006 Å
α	90°
β	117.05 ± 0.02°
γ	90°
Cell volume	2809.7 ± 1.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1363
Residual factor for significantly intense reflections	0.0897
Weighted residual factors for significantly intense reflections	0.2042
Weighted residual factors for all reflections included in the refinement	0.2146
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4324247.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4324247.cif
40952	2012-03-09	../uploads/cif-deposit/cod/cif Adding structures of 4324247 via cif-deposit CGI script.	4324247.cif