Crystallography Open Database

Information card for entry 4327233

Preview

Coordinates	4327233.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H108 Cl16 Co4 N24 O32 P8 Zn8
Calculated formula	C24 H106 Cl16 Co4 N24 O32 P8 Zn8
Title of publication	Syntheses and Characterizations of Three Low-Dimensional Chloride-Rich Zincophosphates Assembled about [d-Co(en)3]3+ and [dl-Co(en)3]3+ Complex Cations
Authors of publication	Peng Chen; Jiyang Li; Fangzheng Duan; Jihong Yu; Ruren Xu; Raj Pal Sharma
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	6683 - 6687
a	31.103 ± 0.006 Å
b	9.0456 ± 0.0018 Å
c	16.499 ± 0.003 Å
α	90°
β	100.43 ± 0.03°
γ	90°
Cell volume	4565.2 ± 1.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	5
Hermann-Mauguin space group symbol	C 1 2 1
Hall space group symbol	C 2y
Residual factor for all reflections	0.1685
Residual factor for significantly intense reflections	0.086
Weighted residual factors for significantly intense reflections	0.1732
Weighted residual factors for all reflections included in the refinement	0.2434
Goodness-of-fit parameter for all reflections included in the refinement	0.81
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179375 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/72.	4327233.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327233.cif
60949	2012-06-20	cif/ Adding structures of 4327233 via cif-deposit CGI script.	4327233.cif