Crystallography Open Database

Information card for entry 4327314

Preview

Coordinates	4327314.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H56 N4 O V
Calculated formula	C37 H49 N4 O V
Title of publication	Dinitrogen Partial Reduction by Formally Zero- and Divalent Vanadium Complexes Supported by the Bis-iminopyridine System
Authors of publication	Indu Vidyaratne; Sandro Gambarotta; Ilia Korobkov; Peter H. M. Budzelaar
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	1187 - 1189
a	25.093 ± 0.004 Å
b	11.7898 ± 0.0018 Å
c	30.183 ± 0.005 Å
α	90°
β	112.754 ± 0.003°
γ	90°
Cell volume	8234 ± 2 Å³
Cell temperature	208 ± 2 K
Ambient diffraction temperature	208 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0999
Residual factor for significantly intense reflections	0.0634
Weighted residual factors for significantly intense reflections	0.1568
Weighted residual factors for all reflections included in the refinement	0.1714
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327314.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327314.cif
61078	2012-06-21	cif/ Adding structures of 4327314 via cif-deposit CGI script.	4327314.cif