Crystallography Open Database

Information card for entry 4327393

Preview

Coordinates	4327393.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H42 Cl4 N10 O6 Pd2
Calculated formula	C42 H42 Cl4 N10 O6 Pd2
Title of publication	Macrocyclic and Lantern Complexes of Palladium(II) with Bis(amidopyridine) Ligands: Synthesis, Structure, and Host-Guest Chemistry
Authors of publication	Nancy L. S. Yue; Dana J. Eisler; Michael C. Jennings; Richard J. Puddephatt
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	7671 - 7681
a	23.6322 ± 0.0004 Å
b	8.4044 ± 0.0001 Å
c	22.9866 ± 0.0003 Å
α	90°
β	97.932 ± 0.001°
γ	90°
Cell volume	4521.79 ± 0.11 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0736
Residual factor for significantly intense reflections	0.0503
Weighted residual factors for significantly intense reflections	0.1199
Weighted residual factors for all reflections included in the refinement	0.1328
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179376 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/73.	4327393.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327393.cif
61164	2012-06-25	cif/ Adding structures of 4327393 via cif-deposit CGI script.	4327393.cif