Crystallography Open Database

Information card for entry 4329039

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Structure parameters

Formula	C54 H60 Ag4 F12 N20 O16 S4
Calculated formula	C54 H60 Ag4 F12 N20 O16 S4
Title of publication	Sensitivity of Silver(I) Complexes of a Pyrimidine-Hydrazone Ligand to Solvent, Counteranion, and Metal-to-Ligand Ratio Changes
Authors of publication	Daniel J. Hutchinson; Scott A. Cameron; Lyall R. Hanton; Stephen C. Moratti
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	5070 - 5081
a	8.834 ± 0.005 Å
b	12.8072 ± 0.001 Å
c	15.3793 ± 0.0012 Å
α	97.165 ± 0.004°
β	92.266 ± 0.004°
γ	95.012 ± 0.004°
Cell volume	1717.6 ± 1 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0283
Residual factor for significantly intense reflections	0.0261
Weighted residual factors for significantly intense reflections	0.0648
Weighted residual factors for all reflections included in the refinement	0.0663
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301838 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 4/32/ Each referenced PubChem compound corresponds to the full crystal structure.	4329039.cif
179393	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/90.	4329039.cif
78079	2013-04-01	cif/ Adding structures of 4329039 via cif-deposit CGI script.	4329039.cif