Crystallography Open Database

Information card for entry 4330147

Preview

Coordinates	4330147.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C80 H73 Ge Ir O2 P4 Rh Si
Calculated formula	C80 H73 Ge Ir O2 P4 Rh Si
Title of publication	Mixed Bis(μ-silylene) and (μ-Silylene)/(μ-Germylene) Complexes Involving the Rh/Ir Metal Combination: Nature of the Si...Si Interactions in the Bis(μ-silylene) Species
Authors of publication	Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	9249 - 9258
a	20.1747 ± 0.0007 Å
b	22.4687 ± 0.0008 Å
c	30.2707 ± 0.0011 Å
α	90°
β	96.4467 ± 0.0005°
γ	90°
Cell volume	13634.9 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.034
Residual factor for significantly intense reflections	0.0247
Weighted residual factors for significantly intense reflections	0.06
Weighted residual factors for all reflections included in the refinement	0.0677
Goodness-of-fit parameter for all reflections included in the refinement	1.088
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179404 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/01.	4330147.cif
79397	2013-04-05	cif/ Adding structures of 4330147 via cif-deposit CGI script.	4330147.cif