Crystallography Open Database

Information card for entry 4331486

Preview

Coordinates	4331486.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Cs4Pb4Ge5S16
Formula	Cs4 Ge5 Pb4 S16
Calculated formula	Cs4 Ge5 Pb4 S16
Title of publication	Exploratory Synthesis in Molten Salts: Role of Flux Basicity in the Stabilization of the Complex Thiogermanates Cs4Pb4Ge5S16, K2PbGe2S6, and K4Sn3Ge3S14
Authors of publication	Palchik, Oleg; Marking, Gregory M.; Kanatzidis, Mercouri G.
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Journal issue	12
Pages of publication	4151 - 4153
a	38.302 ± 0.0019 Å
b	9.077 ± 0.0005 Å
c	19.4421 ± 0.0001 Å
α	90°
β	90°
γ	90°
Cell volume	6759.4 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	64
Hermann-Mauguin space group symbol	C m c a
Hall space group symbol	-C 2ac 2
Residual factor for all reflections	0.0416
Residual factor for significantly intense reflections	0.0249
Weighted residual factors for significantly intense reflections	0.0584
Weighted residual factors for all reflections included in the refinement	0.0636
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179417 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/14.	4331486.cif
97647	2014-01-29	cif/ Adding structures of 4331486 via cif-deposit CGI script.	4331486.cif