Crystallography Open Database

Information card for entry 4332275

Preview

Coordinates	4332275.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	phosphine
Chemical name	Diphenyl[2-(1-phenylhydrazo)phenyl]phosphine
Formula	C24 H21 N2 P
Calculated formula	C24 H21 N2 P
SMILES	P(c1ccccc1NNc1ccccc1)(c1ccccc1)c1ccccc1
Title of publication	Systematic Study on the Structures and Reactivity of Hydrazobenzenes and Azobenzenes Bearing a Chalcogenophosphoryl Group
Authors of publication	Yamamura, Masaki; Kano, Naokazu; Kawashima, Takayuki
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	16
Pages of publication	6497 - 6507
a	30.598 ± 0.016 Å
b	7.779 ± 0.003 Å
c	22.26 ± 0.011 Å
α	90°
β	133.846 ± 0.005°
γ	90°
Cell volume	3821 ± 3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0435
Residual factor for significantly intense reflections	0.0322
Weighted residual factors for significantly intense reflections	0.0714
Weighted residual factors for all reflections included in the refinement	0.0765
Goodness-of-fit parameter for all reflections included in the refinement	0.974
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179425 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/22.	4332275.cif
98206	2014-01-29	cif/ Adding structures of 4332275, 4332276, 4332277, 4332278, 4332279, 4332280, 4332281, 4332282 via cif-deposit CGI script.	4332275.cif