Crystallography Open Database

Information card for entry 4332328

Preview

Coordinates	4332328.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Compound X
Formula	C32.5 H33 N2 O7.5 U
Calculated formula	C32.5 H33 N2 O7.5 U
Title of publication	Crystal Structure of a CsF−Uranyl−Salen Complex. An Unusual Cesium−Chlorine Coordination
Authors of publication	Cametti, Massimo; Nissinen, Maija; Dalla Cort, Antonella; Rissanen, Kari; Mandolini, Luigi
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	16
Pages of publication	6099 - 6101
a	10.0159 ± 0.0005 Å
b	10.4519 ± 0.0004 Å
c	15.2798 ± 0.0007 Å
α	103.338 ± 0.002°
β	95.853 ± 0.002°
γ	104.6 ± 0.003°
Cell volume	1484.23 ± 0.12 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0514
Residual factor for significantly intense reflections	0.0451
Weighted residual factors for significantly intense reflections	0.1189
Weighted residual factors for all reflections included in the refinement	0.1225
Goodness-of-fit parameter for all reflections included in the refinement	1.142
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4332328.cif
98239	2014-01-29	cif/ Adding structures of 4332327, 4332328 via cif-deposit CGI script.	4332328.cif