Crystallography Open Database

Information card for entry 4333084

Preview

Coordinates	4333084.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	tetra-n-butylbis(methanesulfonato)bis(hydrogenmethylphosphonato)ditin
Formula	C20 H50 O12 P2 S2 Sn2
Calculated formula	C20 H50 O12 P2 S2 Sn2
Title of publication	Expanding the Scope of Sulfur-Centered Arbuzov Rearrangement in Diethyl/Di-n-propyl Sulfite for the Synthesis of Mixed-Ligand Di-n-butyltin Alkanesulfonates†
Authors of publication	Shankar, Ravi; Singh, Atul Pratap; Upreti, Shailesh
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	23
Pages of publication	9166 - 9168
a	10.74 ± 0.0019 Å
b	9.9175 ± 0.0017 Å
c	16.864 ± 0.003 Å
α	90°
β	92.678 ± 0.003°
γ	90°
Cell volume	1794.3 ± 0.5 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0288
Residual factor for significantly intense reflections	0.0262
Weighted residual factors for significantly intense reflections	0.0715
Weighted residual factors for all reflections included in the refinement	0.073
Goodness-of-fit parameter for all reflections included in the refinement	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179433 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/30.	4333084.cif
98757	2014-01-30	cif/ Adding structures of 4333084 via cif-deposit CGI script.	4333084.cif