Crystallography Open Database

Information card for entry 4334326

Preview

Coordinates	4334326.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C112.5 H96 Cl2 Co2 N2 Si2
Calculated formula	C112.5 H96 Cl2 Co2 N2 Si2
Title of publication	Extremely Bulky Amido First Row Transition Metal(II) Halide Complexes: Potential Precursors to Low Coordinate Metal-Metal Bonded Systems
Authors of publication	Jamie Hicks; Cameron Jones
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	3900 - 3907
a	13.3383 ± 0.0007 Å
b	18.1137 ± 0.0008 Å
c	19.0342 ± 0.0011 Å
α	90°
β	99.164 ± 0.005°
γ	90°
Cell volume	4540.1 ± 0.4 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0818
Residual factor for significantly intense reflections	0.0605
Weighted residual factors for significantly intense reflections	0.1599
Weighted residual factors for all reflections included in the refinement	0.1802
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4334326.cif
100144	2014-02-04	cif/ Adding structures of 4334326 via cif-deposit CGI script.	4334326.cif