Crystallography Open Database

Information card for entry 4334462

Preview

Coordinates	4334462.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74 H70 N2 O22 P2 Pt12
Calculated formula	C74 H70 N2 O22 P2 Pt12
Title of publication	PPh3-Derivatives of [Pt3n(CO)6n]2- (n= 2-6) Chini's Clusters: Syntheses, Structures, and 31P NMR Studies
Authors of publication	Iacopo Ciabatti; Cristina Femoni; Maria Carmela Iapalucci; Giuliano Longoni; Tatiana Lovato; Stefano Zacchini
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	4384 - 4395
a	15.5382 ± 0.0013 Å
b	20.7765 ± 0.0017 Å
c	27.887 ± 0.003 Å
α	90°
β	105.53 ± 0.001°
γ	90°
Cell volume	8674.1 ± 1.4 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1094
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.0865
Weighted residual factors for all reflections included in the refinement	0.1074
Goodness-of-fit parameter for all reflections included in the refinement	0.996
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179447 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/44.	4334462.cif
100289	2014-02-04	cif/ Adding structures of 4334462 via cif-deposit CGI script.	4334462.cif