Crystallography Open Database

Information card for entry 4335361

Preview

Coordinates	4335361.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H64 N6 O16 P2 Pd6
Calculated formula	C30 H60 N6 O16 P2 Pd6
Title of publication	Facile Formation of Stable Tris(imido)phosphate Trianions as Their Tri- and Hexanuclear Pd(II) Complexes in Protic Solvents
Authors of publication	Arvind K. Gupta; S. Arun Dixith Reddy; Ramamoorthy Boomishankar
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	7608 - 7614
a	14.8019 ± 0.0016 Å
b	18.678 ± 0.002 Å
c	38.14 ± 0.004 Å
α	90°
β	90.015 ± 0.004°
γ	90°
Cell volume	10544.6 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0589
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.0948
Weighted residual factors for all reflections included in the refinement	0.0988
Goodness-of-fit parameter for all reflections included in the refinement	1.108
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179456 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/53.	4335361.cif
101287	2014-02-11	cif/ Adding structures of 4335361 via cif-deposit CGI script.	4335361.cif