Crystallography Open Database

Information card for entry 4335563

Preview

Coordinates	4335563.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H70 Cl9 Cu8 Dy3 N6 O28
Calculated formula	C54 H69.996 Cl9 Cu8 Dy3 N6 O28
Title of publication	Lanthanide Triangles Sandwiched by Tetranuclear Copper Complexes Afford a Family of Hendecanuclear Heterometallic Complexes [LnIII3CuII8] (Ln = La-Lu): Synthesis and Magnetostructural Studies
Authors of publication	Olga Iasco; Ghenadie Novitchi; Erwann Jeanneau; Dominique Luneau
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	8723 - 8731
a	22.089 ± 0.002 Å
b	22.089 ± 0.002 Å
c	20.674 ± 0.003 Å
α	90°
β	90°
γ	120°
Cell volume	8735.9 ± 1.7 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	7
Space group number	155
Hermann-Mauguin space group symbol	R 3 2 :H
Hall space group symbol	R 3 2"
Residual factor for all reflections	0.0969
Residual factor for significantly intense reflections	0.0803
Weighted residual factors for all reflections	0.2125
Weighted residual factors for significantly intense reflections	0.1866
Weighted residual factors for all reflections included in the refinement	0.2125
Goodness-of-fit parameter for all reflections included in the refinement	0.8977
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179458 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/55.	4335563.cif
101496	2014-02-14	cif/ Adding structures of 4335563 via cif-deposit CGI script.	4335563.cif