Crystallography Open Database

Information card for entry 4338689

Preview

Coordinates	4338689.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C108 H100 Ag4 N12 O4 P4 S4
Calculated formula	C108 H100 Ag4 N12 O4 P4 S4
Title of publication	Factors involved in the nuclearity of silver thiosemicarbazone clusters: cocrystallization of two different sized tetranuclear silver(I) clusters derived from a phosphinothiosemicarbazone ligand.
Authors of publication	Castiñeiras, Alfonso; Pedrido, Rosa
Journal of publication	Inorganic chemistry
Year of publication	2008
Journal volume	47
Journal issue	13
Pages of publication	5534 - 5536
a	14.4071 ± 0.0003 Å
b	16.1237 ± 0.0003 Å
c	22.0432 ± 0.0005 Å
α	87.155 ± 0.001°
β	86.775 ± 0.001°
γ	78.752 ± 0.001°
Cell volume	5010.32 ± 0.18 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0541
Residual factor for significantly intense reflections	0.0378
Weighted residual factors for significantly intense reflections	0.0964
Weighted residual factors for all reflections included in the refinement	0.1022
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179489 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/86.	4338689.cif
115417	2014-06-03	cif/ Adding structures of 4338689 via cif-deposit CGI script.	4338689.cif