Crystallography Open Database

Information card for entry 4339229

Preview

Coordinates	4339229.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H73 N7 O31 Pb6
Calculated formula	C69 H66 N7 O31 Pb6
Title of publication	Organic-acid effect on the structures of a series of lead(II) complexes.
Authors of publication	Yang, Jin; Ma, Jian-Fang; Liu, Ying-Ying; Ma, Ji-Cheng; Batten, Stuart R.
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6542 - 6555
a	11.1446 ± 0.0015 Å
b	16.3388 ± 0.0015 Å
c	43.989 ± 0.005 Å
α	90°
β	90.16 ± 0.01°
γ	90°
Cell volume	8009.9 ± 1.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1142
Residual factor for significantly intense reflections	0.0827
Weighted residual factors for significantly intense reflections	0.1594
Weighted residual factors for all reflections included in the refinement	0.1708
Goodness-of-fit parameter for all reflections included in the refinement	1.11
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179495 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/92.	4339229.cif
117216	2014-06-14	cif/ Adding structures of 4339221, 4339222, 4339223, 4339224, 4339225, 4339226, 4339227, 4339228, 4339229, 4339230 via cif-deposit CGI script.	4339229.cif